Calibrating the Iowa pore index with mercury intrusion porosimetry and petrography.
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2017-10-31
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Abstract:The Iowa Pore Index (IPI) test is a fast, non-destructive, inexpensive, and environmentally friendly test used by several
Midwestern state departments of transportation to determine the volume ratio of macropores to micropores in a coarse rock
aggregate. When combined with x-ray diffraction and x-ray fluorescence, this method has been shown to be effective in
predicting the performance of aggregates in portland cement concrete. The test has the potential to replace mercury porosimetry
and be integrated into any petrophysical laboratory.
This research aimed to understand the geological factors (depositional environment, facies, grain and pore types, texture, and
paragenesis) responsible for the results of the IPI test. Samples of various geologic ages were collected around Iowa to represent
different combinations of accepted and rejected porosity and clay contents. The pore index of each sample was calibrated
quantitatively via helium and mercury porosimetry and qualitatively via thin section petrography.
The findings show that even the most homogeneous sources have at least three different rock types. Petrographic analysis showed
that limestones with a sparite matrix, peloidal grains, and a low matrix-to-allochem ratio (i.e., grainy) are better for road
construction than limestones with a micrite matrix, skeletal grains, and a high matrix-to-allochem ratio (i.e., muddy). Dolostones
with fine to coarse grains, crystal-supported euhedral to subhedral rhombs, and porous intercrystalline areas are more desirable
than dolostones with very fine grains and a tightly interlocking crystal mosaic in anhedral form.
Several linear models were developed to relate IPI to helium porosity. Limestones with a helium porosity less than ~7% and
dolostones with a helium porosity greater than ~13% were found to be desirable for use in road construction. The critical range of
pore-throat size was found to be between 0.02 and 0.1 µm. Coarse aggregates with modal pore throat sizes above this range were
found to be desirable for use in road construction
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