Improved infra-red procedure for the evaluation of calibrating units.
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2011-01-04
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NTL Classification:AGR-SAFETY AND SECURITY-SAFETY AND SECURITY;NTL-SAFETY AND SECURITY-SAFETY AND SECURITY;NTL-SAFETY AND SECURITY-Highway Safety;
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Abstract:Introduction. The NHTSA Model Specifications for Calibrating Units for Breath
Alcohol Testers (FR 72 34742-34748) requires that calibration units submitted for
inclusion on the NHTSA Conforming Products List for such devices be evaluated using
one of three alternate procedures, all of which were developed at the Volpe Center. The
first uses gas chromatography and wet gas reference samples for evaluation. This
procedure is no longer used because of the advent of dry gas CUs on the market. Gas
chromatography is an inappropriate technique for evaluation of dry gases using wet gas
reference samples. A second alternative uses gas chromatography with dry gas reference
samples. The dry gas references were obtained from the National Institute for Science
and Technology. A third procedure uses a non-dispersive infra-red spectrophotometry.
This third procedure is the preferred one, since reference samples are prepared at the
Volpe Center so that reliance on outside sources for reference samples is not necessary.
This preferred procedure uses a National Patent Analytical Systems, Inc. Datamaster
breath alcohol analyzer instrument to analyze samples. This device is a non-dispersive
infra-red spectrophotometer designed for breath (ethyl) alcohol analysis and is listed on
the NHTSA Conforming Products List for evidential breath testers. Analysis is based on
the absorption of a band of infra-red radiation centered at 3.4 microns, a wavelength area
that is strongly absorbed by alcohol and which at the same time is not interfered with by
other possible substances found in human breath, other than acetone.
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